摘要
以甘草酸为原料通过水热法合成了甘草次酸甲酯,并通过红外光谱和1H核磁共振等手段对其进行表征,确定了其化学结构.该合成方法具有简便、快速、收率高等优点.
Methyl glycyrrhetate has been synthesized successfully by hydrothermal method with Glycyrrhizic acid.The samples were characterized by fourier transform infrared（FT-IR） and 1 H NMR techniques et al.Hydrothermal method has opened up new approach and method for the research into composing glycyrrhetinic acid derivative,that the method is simple and convenient,rapid and high collecting rates.
出处
《东北师大学报（自然科学版）》
CAS
CSCD
北大核心
2007年第4期154-156,共3页
Journal of Northeast Normal University(Natural Science Edition)
基金
吉林省科技发展计划项目(20011109)
关键词
甘草酸
甘草次酸
甘草次酸甲酯
水热法
化学位移
核磁共振
Glycyrrhizic acid
glycyrrhetinic acid
methyl glycyrrhetate
hydrothermal method
chemistry-shift
NMR
