摘要
采用微波消解-端视等离子体发射光谱(ICP-AES)测定蜂产品中重金属微量元素铅、镉、砷,并对ICP-AES工作参数及条件进行了优化和选择,Pb、Cd、As的检出限分别为2.9×10-3mg/L、0.056×10-3mg/L、5.2×10-3mg/L,线性范围为0～500μg/L,相对标准偏差范围为2.9%～8.5%;回收率范围为91%～102%。该方法与国标法比较,结果无显著性差异,能满足蜂产品测定要求。
A method of microwave digestion axial-view ICP-AES was applied to determine heave metals trace elements lead, arseic, cadmium in honey products. Operation parameters of ICP-AES and condition were optimized and selected. The detection limit was Pb： 2.9-03 mg/L, As： 5.2-103 mg/L, Cd： 0.056-103 mg/L.The RSD was in the range of 2.9 %-8.5 % and the recovery was in the range of 91%-102 %.This method was compared with the national standard way and their resuhes showed no significant difference from that of the national standard way .The resuhe was satisfactory for honey products.
出处
《食品研究与开发》
CAS
北大核心
2007年第11期130-133,共4页
Food Research and Development
