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手性4-苯基-2-噁唑烷酮的合成研究 被引量:1

Preparation of (S)-(+)-4-Phenyl-2-oxazolidinone
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摘要 从L-苯甘氨酸出发,经过酯化、还原、缩合三步合成(S)-(+)-4-苯基-2-噁唑烷酮总收率达到了70%。目标产物的结构经过IR、HNMR和MS确证。 The synthetic methods on (S)-(+)-4-Phenyl-2-oxazolidinone is described in detail. Using L- phenylglycine as materials, (S)-(+)-4-Phenyl-2-oxazoli -dinone is synthesized by three steps of esterification, reduction and condensation. The product yield is 70%. The structures of the products were determined by IR, 1H-NMR, and MS.
出处 《浙江化工》 CAS 2007年第7期3-4,共2页 Zhejiang Chemical Industry
关键词 噁唑烷酮 L-苯甘氨酸 合成 oxazolidinone L- phenylglycine synthesis
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