摘要
目的:建立羚羊感冒片中牛蒡苷的含量测定方法。方法:采用HPLC法,色谱柱为KF-C18(4.6mm×250mm);流动相为乙腈-水(25:75);检测波长为280nm。结果:牛蒡苷在0.8~1.6μg范围内线性良好。加样回收率为99.93%,RSD%为0.23%(n=5).结论:方法简便,可行,重现性良好,结果准确,可加强羚羊感冒片的质量控制。
Objective:To establish a detemaination method of Arctiin in Lingyang Ganmao Tablets.Methods:The content of Arctiin was determined by HPLC.With acetonitrile-water( 25: 75)as mobile phase, detection wavelength at 280nm. Results :The linear range was between 0.8- 1.6μg of Arctiin.The mean recovery was 99.93 %, RSD% = 0.23% (n= 5).Conclusion:The method is simple, accurate and reliable and can be used for quality control of Lingyang Ganmao Tabets.
出处
《黑龙江医药》
CAS
2007年第4期299-300,共2页
Heilongjiang Medicine journal