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丙酮-硫酸铵双水相体系分离纯化红花红色素 被引量:22

Separation and purification of carthamine from carthamus tinctorius by acetone-ammonium sulfate aqueous two-phase system
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摘要 A kind of simple aqueous two-phase system composed of acetone,inorganic salt and water was used to separate and purify carthamine from safflower petals.Experimental results show that(NH4)2SO4 has the stronger phases-forming ability than K2HPO4 and NaCl.The optimum conditions for isolating carthamine from safflower yellow were chose as V(CH3)2CO=5mL,VH2O=5mL,m(NH4)2SO4=2.5g.Under the conditions,the yield can reach to 99 % for the extraction of carthamine with the partition coefficient K>55.The carthamine product with high purity was obtained using analog counter-current extracting experiment. A kind of simple aqueous two - phase system composed of acetone, inorganic salt and water was used to separate and purify carthamine from safflower petals. Experimental results show that (NH4 )2SO4 has the stronger phases -forming ability than K2 HPO4 and NaCl. The optimum conditions for isolating carthamine from safflower yellow were chose as V( CH3 )2 CO = 5mL, VH2O =5mL,m(NH4)2SO4 =2.5g. Under the conditions, the yield can reach to 99 % for the extraction of carthamine with the partition coefficient K 〉 55. The earthamine product with high purity was obtained using analog counter - current extracting experiment .
出处 《化学研究与应用》 CAS CSCD 北大核心 2007年第6期679-682,共4页 Chemical Research and Application
基金 四川省科技厅攻关课题 项目编号:06(05SG022-021-04)
关键词 红花 红色素 双水相 safflower Carthamine aqueous two- phase
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