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FTIR监测7-氟-2H-1,4-苯并噁嗪-3(4H)-酮的固相合成 被引量:1

Monitoring of Solid-phase Synthesis of 7-Fluoro-2H-1,4-benzoxazine-3(4H)-ones via FTIR Spectroscopy
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摘要 The solid-phase synthesis of 7-fluoro-1,4-2H-benzoxazine 3(4H)-ones on Wang resin via esterification,etherification,reduction,cyclization and cleavage reactions was studied,and the reaction conditions were optimized after analyzing the reaction kinetics according to the IR spectrum. The solid-phase synthesis of 7-fluoro-1,4-2H-benzoxazine 3 (4H)-ones on Wang resin via esterification, etherification, reduction, cyclization and cleavage reactions was studied, and the reaction conditions were optimized after analyzing the reaction kinetics according to the IR spectrum.
出处 《高等学校化学学报》 SCIE EI CAS CSCD 北大核心 2006年第11期2117-2119,共3页 Chemical Journal of Chinese Universities
基金 国家自然科学基金(批准号:20372021 B20572019)资助
关键词 组合化学 固相有机合成 红外光谱 Combinatorial chemistry Solid-phase organic synthesis Infrared spectroscopy
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