摘要
气相色谱法同时测定土壤中多种有机氯及拟除虫菊酯类农药。对土壤的分析结果：有机氯农药的检出限0．001～0、003μg／mL，拟除虫菊酯类农药检出限0.008～0．02μg／mL，线性相关系数0．9978～0．9999。用y（石油醚）：V（丙酮）=3：1超声波提取，有机氯农药回收率94．2％～124．0％，相对标准偏差为3．3％～8．8％（n=5）；拟除虫菊酯类农药回收率95．2％～118．3％，相对标准偏差为5．7％～7．1％（n=5）；方法适用于土壤样品中农药残留测定。
A method for the determination of organochlorine and pyrethroid pesticides in soil samples was developed. The results of monitoring the quaihy of soil were as follows： The detection limits of organochlorine pesticides were 0. 001 -0.003 μg/mL, the detection limits of pyrethroid pesticides were 0.008 -0.02μg/mL, correlation coefficients were 0.9978 - 0. 9999. Using petroleum ether ＋ acetone （3 ： 1 ） as on eluent, the recoveries obtained for organochlo- rine pesticides ranged from 94.2.0 % to 124.0 % and the recoveries of pyrethroid pesticide were 95.2 % - 118.3 %, and with RSD of 3.3 % - 8.8 % and 5.7 % - 7.1% respectively （ n = 5）. Satisfactory results were obtained for the determination of organochlorine and pyrethriod pesticides in soil samples.
出处
《分析试验室》
CAS
CSCD
北大核心
2006年第9期60-63,共4页
Chinese Journal of Analysis Laboratory
