摘要
目的:建立独活寄生合剂(独活、桑寄生、秦艽等)的质量标准。方法:采用TLC对处方中的药材进行了鉴别;用薄层扫描法测定蛇床子素的含量。结果:在TLC图谱中可检出川芎、当归、防风、秦艽、杜仲、细辛、白芍的特征色谱;蛇床子素在0.466~3.600μg间线性关系良好,r=0.9992,平均回收率为95.4%。结论:所建方法可行,重现性好,可用于本品的质量控制。
AIM: To establish the quality standard for Duhuo Jisheng Mixture (Radix Angelicae Pubescentis, Herba Taxilli, Cortex Fraxini, etc. ) METHODS: Herbs in Duhuo Jisheng Mixture were identified by TLC, and osthol content was determined by TLCS. RESULTS: Rhizoma Chuanxiong; Radix Angelicae Sinensis; Radix Saposhnikoviae ; Radix Gentianae Macrophyllae ; Cortex Eucommiae ; Herba Asari ; Radix Paeoniae Alba could be determined. Osthol showed a good linear relationship at a range of 0. 466 - 3. 600 μg, r = 0.999 2. The average recovery was 95.4%. CONCLUSION:The methods are available with a reproducibility and can control the quality of this mixture.
出处
《中成药》
CAS
CSCD
北大核心
2006年第9期1284-1288,共5页
Chinese Traditional Patent Medicine
关键词
独活寄生合剂
独活
桑寄生
蛇床子素
质量标准
Duhuo Jisheng Mixture
Radix Angelicae pubescentis
Herba Taxilli
osthol
quality standard