摘要
本文研究了用浓硝酸将2-乙基蒽醌中的硫定量转化成硫酸根,然后用硫酸钡分光光度比浊法间接测定其硫含量的方法。建立的方法简单、快速、实用。试样分析结果表明准确度及精密度均符合要求。
An analytic method was studied and developed to determine the sulfur impurity in catalyst 2-EAQ.The sample was oxidized with concentrated nitric acid, converting sulfure into sulfate,pricipited with barium chloride,the resultant turbidity of barium sulfate was determined with a spectroscope,sulfur content was calculated. This method is simple and fast,yielding accurate result.
出处
《光谱实验室》
CAS
CSCD
1996年第6期53-55,共3页
Chinese Journal of Spectroscopy Laboratory
关键词
硫
硫酸钡
乙基蒽酯
催化剂
分光光度比浊法
Sulfur,Concentrated Nitric Acied,Barium Sulfate Turbidity,2-EAQ.