摘要
以间二甲酚和氯气为原料,在三氯化铝的催化下合成了对氯间二甲酚,最佳工艺条件为:四氯化碳70 mL,60℃下通氯反应90 m in,收率可以达61.1%。
Chloroxylenol was prepared from 3,5-xylenol and chlorine by using aluminum chloride as catalyst. The optimum synthetic conditions were found as follows：carbon tetrachloride is 70 mL, reaction time is 90min,reaction temperature is 60℃ ,the chloroxylenol yield may reach 61. 1%.
出处
《应用化工》
CAS
CSCD
2006年第2期99-100,103,共3页
Applied Chemical Industry
基金
山西省科技厅攻关项目(041058)
关键词
间二甲酚
氯化
对氯间二甲酚
三氯化铝
3,5-xylenol
chlorination
chloroxylenol
aluminum chloride
