摘要
目的:研究薄荷油β-环糊精包合物的最佳制备工艺。方法:用正交实验法研究配比、温度、时间三个因素对薄荷油β-环糊精包合物的饱和水溶液法的制备工艺的影响,考察包合物的收率,并用TLC、显微影像验证包合物的形成。结果:最佳的工艺条件薄荷油2.5 m l,包合温度50℃,包合时间3.5 h。结论:此方法可用于制备薄荷油β-环糊精包合物。
Objective：To study optimum inclusion process for β-eyelodextrin inclusion compound of Pennyroyal. Methods：The preparation procedure of β-eyelodextrin inclusion compound of pennyroyal was studied by orthogonal test with 3 factors： Pennyroyal, temperature and time. The inclusion compound was proved by thin layer chromatography and microscope. Results：The optimum preparation conditions for inclusion compound were established as ： pennyroyal 2.5 ml , inclusion temperature was at 50℃ and for 3.5hr. Conclusion：Tbe method can be used for preparation of the inclusion compound.
出处
《时珍国医国药》
CAS
CSCD
北大核心
2005年第12期1270-1271,共2页
Lishizhen Medicine and Materia Medica Research
