摘要
选定了氯化亚砜氯化三氯乙酸法,通过试验确定了其优惠工艺条件。按该条件可制得纯度为98%的三氯乙酰氯,收率可达91%。
A desired reaction's condition of trichloroacetyl acid with thionylchloride was found.The yield of the reaction which was carried out in this condition is about 90%,and purity 98%.
出处
《湖南化工》
1995年第4期32-33,42,共3页