摘要
以七水合硫酸锌和十二水合磷酸钠为原料,乙二胺为模板剂,通过室温固相反应合成了磷酸锌微孔化合物。对产物进行了元素分析,用IR,XRD分析基团结构及微孔特征,用TG-DTA分析热稳定性。分析结果表明:产物为包含有模板剂乙二胺,且具有空旷微孔结构的磷酸锌晶体。
Zinc phosphate with microporous structure was synthesized by solid-state reaction at room temperature when ZnSO_4·7H_(2)O and Na_3PO_4·12H_2O were chosen as raw materials, ethylenediamine as template agent.The obtained samples were characterized by means of element analysis,IR,TG-DTA and XRD.The results show that the product is zincphosphate-crystal with template agent ethylenediamine and the materials structures is open-frameworks.
出处
《无机盐工业》
CAS
北大核心
2005年第5期21-22,共2页
Inorganic Chemicals Industry
基金
广西教育厅科研项目(桂教科研字 2002第 316号)。
关键词
磷酸锌
微孔材料
固相反应
zinc phosphate,microporous material,solid-state reaction
