摘要
建立通栓醒脑注射液中冰片和麝香酮含量的测定方法.采用固相萃取法处理样品,用GC-MS法同时分离测定冰片和麝香酮的含量.冰片和麝香酮的回收率和相对标准偏差分别为97.8%～104.8%,2.72%和97.6%～105.4%,3.86%.本法快速准确,可用于通栓醒脑注射液的质量控制.
An assay methods for measuring borneol and muscone in Tongshuanxingnao injections was estabˉlished.Borneol and muscone were extracted with a solid-phase extraction procedure and were simultaneously measured with GC-MS method after a solid-phase extraction procedure.The recoveries and relative standard deviation were97.8%～104.8%and2.72%for borneol and97.6%～105.4%and3.86%for muscone,respectively.The method was simple and accurate and can be used for the quality control of Tongshuanxingˉnao injections.
出处
《分析测试学报》
CAS
CSCD
北大核心
2005年第2期104-105,108,共3页
Journal of Instrumental Analysis
