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碘氧化法测定中药五倍子中的单宁 被引量:3

Determination of Tannic Acid in Chinese Gall Nut via Oxidation with I_2
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摘要 Oxidation reaction of tannic acid by I 2 was used in the determination of tannic acid in Chinese gall nut by ultraviolet spectrophotometry in aqueous ethanol solution, where I 2 exhibits a sensitive absorption at 289 nm. The linear regression equation of the method is A=0.018 61+0.245 3c(mg/L) with a correlation coefficient of 0.999 8. The linear response range is 0.0~2.0 mg/L, the apparent molar absorptivity is 4.14× 10 5 L/(mol·cm) and the recovery is in the range of 97.8%~104.3%. The method has the advantages of simplicity, high sensitivity and rapidity. Oxidation reaction of tannic acid by I 2 was used in the determination of tannic acid in Chinese gall nut by ultraviolet spectrophotometry in aqueous ethanol solution, where I 2 exhibits a sensitive absorption at 289 nm. The linear regression equation of the method is A=0.018 61+0.245 3c(mg/L) with a correlation coefficient of 0.999 8. The linear response range is 0.0~2.0 mg/L, the apparent molar absorptivity is 4.14× 10 5 L/(mol·cm) and the recovery is in the range of 97.8%~104.3%. The method has the advantages of simplicity, high sensitivity and rapidity.
出处 《应用化学》 CAS CSCD 北大核心 2005年第2期227-229,共3页 Chinese Journal of Applied Chemistry
关键词 单宁 五倍子 碘氧化 紫外分光光度法 tannic acid,Chinese gall nut,iodine oxidation,ultraviolet spectrophotometry
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