摘要
采用研磨法制备了大蒜素-β-环糊精包合物,用正交设计对包合物制备条件进行了优化.大蒜素-β-环糊精包合物制备的最佳条件:β-环糊精12g,大蒜素1mL;温度25℃;反应介质pH=6;研磨时间2h.用气相色谱法测定了包合物中大蒜素的含量.
Allicin-β-cyclodextrin inclusion complex was prepared by grinding method and the conditions of preparation were optimized by orthogonal design. The optimal conditions for the preparation were as follows: ratio between β-cyclodextrin and allicin, 12∶1(g∶mL); temperature, 25 ℃;pH=6;grinding time, (2 h.) Allicin in the inclusion complex was determined by gas chromatography.
出处
《北京理工大学学报》
EI
CAS
CSCD
北大核心
2004年第7期650-652,共3页
Transactions of Beijing Institute of Technology
关键词
大蒜素-β-环糊精包合物
研磨法
正交设计
气相色谱
allicin-β-cyclodextrin inclusion complex
grinding method
orthogonal design
gas chromatography
