The growth of proeutectoid ferrite in Fe-0.15%C-0.8 % Mn carbon steel during continuous cooling process was observed in situ and tracked dynamically by using a high temperature confocal scanning laser microscope ( HT...The growth of proeutectoid ferrite in Fe-0.15%C-0.8 % Mn carbon steel during continuous cooling process was observed in situ and tracked dynamically by using a high temperature confocal scanning laser microscope ( HTC SLM), and the growing process was also investigated. The growth regularity of proeutectoid ferrite plates within austenite was obtained by analyzing the growth fashions and directions and quantitatively studying the growth rates. The results show that the proeutectoid ferrite plates grow in the fashion of creeping, twisting, branching off and de flection within austenite grain. The proeutectoid ferrite plates can grow up along preferential orientation but not strictly. Its growth direction fluctuates and changes in a small range. The growth rate also changes with the change in growth fashion and direction. When the proeutectoid ferrite grows in the fashion of deflection, the average growth rate of proeutectoid ferrite before its deflection is about 61.9, and 46.2 μm/s after the 15°deflection. At the begin ning of proeutectoid ferrite growing, there is a fast growing stage. As the tip of proeutectoid ferrite extends forward continuously, the growth rate will slow down. Therefore, it will induce the proeutectoid ferrite to deflect and grow along another favorable direction, then it will grow rapidly again.展开更多
Rod-shaped mesoporous titanosilicate composites (RMTSs) with controllable aspect ratios (ARs) were fabricated using cetyltrimethylammonium bromide (CTAB) and ammonium hydroxide (NH4OH) at a continuous stirring...Rod-shaped mesoporous titanosilicate composites (RMTSs) with controllable aspect ratios (ARs) were fabricated using cetyltrimethylammonium bromide (CTAB) and ammonium hydroxide (NH4OH) at a continuous stirring rate, resulting in ARs ranging from 1 to 5. Slowing the stirring rate or increasing the concentration of CTAB mainly impacted the length growth, whereas NH4OH affected the width growth. Photocatalytic activity studies revealed that the length of RMTSs played a more significant role than the width at lower ARs in their photocatalytic activity.展开更多
基金Item Sponsored by Scientific Director Fund of National Natural Science Foundation of China(51141010)
文摘The growth of proeutectoid ferrite in Fe-0.15%C-0.8 % Mn carbon steel during continuous cooling process was observed in situ and tracked dynamically by using a high temperature confocal scanning laser microscope ( HTC SLM), and the growing process was also investigated. The growth regularity of proeutectoid ferrite plates within austenite was obtained by analyzing the growth fashions and directions and quantitatively studying the growth rates. The results show that the proeutectoid ferrite plates grow in the fashion of creeping, twisting, branching off and de flection within austenite grain. The proeutectoid ferrite plates can grow up along preferential orientation but not strictly. Its growth direction fluctuates and changes in a small range. The growth rate also changes with the change in growth fashion and direction. When the proeutectoid ferrite grows in the fashion of deflection, the average growth rate of proeutectoid ferrite before its deflection is about 61.9, and 46.2 μm/s after the 15°deflection. At the begin ning of proeutectoid ferrite growing, there is a fast growing stage. As the tip of proeutectoid ferrite extends forward continuously, the growth rate will slow down. Therefore, it will induce the proeutectoid ferrite to deflect and grow along another favorable direction, then it will grow rapidly again.
基金supported by the National Natural Science Foundation of China(Nos.20976100,51372124)the Natural Science Foundation of Shandong Province(Nos.ZR2010BM013, ZR2011BQ009)+1 种基金the Program for Scientific Research Innovation Team in Colleges and Universities of Shandong Province(No. 201207)Key Laboratory of Colloid and Surface Chemistry, Ministry of Education(Shandong University,No.201205)
文摘Rod-shaped mesoporous titanosilicate composites (RMTSs) with controllable aspect ratios (ARs) were fabricated using cetyltrimethylammonium bromide (CTAB) and ammonium hydroxide (NH4OH) at a continuous stirring rate, resulting in ARs ranging from 1 to 5. Slowing the stirring rate or increasing the concentration of CTAB mainly impacted the length growth, whereas NH4OH affected the width growth. Photocatalytic activity studies revealed that the length of RMTSs played a more significant role than the width at lower ARs in their photocatalytic activity.