Six new N4-[bi-（4-fluorophenyl）-methyl]-piperazine thiosemicarbazones 3a-f have been prepared starting from [bi-（4-fluorophenyl）-methyl]-piperazine in solvent-free condition under microwave irradiation with excell...Six new N4-[bi-（4-fluorophenyl）-methyl]-piperazine thiosemicarbazones 3a-f have been prepared starting from [bi-（4-fluorophenyl）-methyl]-piperazine in solvent-free condition under microwave irradiation with excellent yields. Their structures have been determined by elemental analysis, IR, MS and 1H NMR data.展开更多
Tetrabenzoporphyrine (H 2TBP) of plane structure and its Co 2+ ,Ni 2+ ,Zn 2+ complexes have been synthesized.The strueture of these complexes were studies by visible spectrum.IR and elemental analysis.
基金Natural Foundation of Southwest University for Nationalities(No.234688).
文摘Six new N4-[bi-（4-fluorophenyl）-methyl]-piperazine thiosemicarbazones 3a-f have been prepared starting from [bi-（4-fluorophenyl）-methyl]-piperazine in solvent-free condition under microwave irradiation with excellent yields. Their structures have been determined by elemental analysis, IR, MS and 1H NMR data.
文摘Tetrabenzoporphyrine (H 2TBP) of plane structure and its Co 2+ ,Ni 2+ ,Zn 2+ complexes have been synthesized.The strueture of these complexes were studies by visible spectrum.IR and elemental analysis.
