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Influencing the Crystallization of Glass-Ceramics by Ultrashort Pulsed Laser Irradiation after Nucleation

Influencing the Crystallization of Glass-Ceramics by Ultrashort Pulsed Laser Irradiation after Nucleation
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摘要 An ultra-fast laser with central wavelength at 1064?nm and 10?ps pulse duration?was used to tightly focus laser radiation?with a microscope objective inside the volume of nucleated Lithium Aluminosilicate (LAS) glass-ceramic. The nonlinear absorption?of the LAS glass-ceramic was measured?for different laser parameters and a thermal simulation was performed to determine the temperature field inside the laser-modified area. After laser processing,?the samples were crystallized in a furnace and the effect of the laser-induced modifications on the microstructure was analyzed with SEM. The SEM analysis shows an increase in the length and size of whisker-shaped?β-spodumene crystals in the laser-modified area. By increasing the dimension of these whisker-shaped crystals, the flexural strength of LAS can be improved locally.?First?four-point bending flexural tests were performed to examine the influence on the mechanical properties. An ultra-fast laser with central wavelength at 1064?nm and 10?ps pulse duration?was used to tightly focus laser radiation?with a microscope objective inside the volume of nucleated Lithium Aluminosilicate (LAS) glass-ceramic. The nonlinear absorption?of the LAS glass-ceramic was measured?for different laser parameters and a thermal simulation was performed to determine the temperature field inside the laser-modified area. After laser processing,?the samples were crystallized in a furnace and the effect of the laser-induced modifications on the microstructure was analyzed with SEM. The SEM analysis shows an increase in the length and size of whisker-shaped?β-spodumene crystals in the laser-modified area. By increasing the dimension of these whisker-shaped crystals, the flexural strength of LAS can be improved locally.?First?four-point bending flexural tests were performed to examine the influence on the mechanical properties.
出处 《New Journal of Glass and Ceramics》 2018年第1期1-11,共11页 玻璃与陶瓷期刊(英文)
关键词 GLASS-CERAMICS Microstructure Nonlinear ABSORPTION PICOSECOND Laser Glass-Ceramics Microstructure Nonlinear Absorption Picosecond Laser
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