摘要
Nanocrystalline Zn(Oxin)2·2H2O (Zinc 8-quinolinolate) was synthesized at near ambient temperature by solid state chemical reaction. Phases, particle sizes and morphology of the prepared nanocrystallite were characterized by Powder X-ray diffraction (XRD) and transmission electron microscopy(TEM). The results showed that the crystallite product had an average size about 30 nm. The effects of a series of reaction conditions on the synthesis of Zn(Oxin)2·2H2O (Zinc 8-quinolinolate) by solid state reaction were studied.
Nanocrystalline Zn(Oxin)2·2H2O (Zinc 8-quinolinolate) was synthesized at near ambient temperature by solid state chemical reaction. Phases, particle sizes and morphology of the prepared nanocrystallite were characterized by Powder X-ray diffraction (XRD) and transmission electron microscopy(TEM). The results showed that the crystallite product had an average size about 30 nm. The effects of a series of reaction conditions on the synthesis of Zn(Oxin)2·2H2O (Zinc 8-quinolinolate) by solid state reaction were studied.
出处
《无机化学学报》
SCIE
CAS
CSCD
北大核心
2004年第7期873-878,共6页
Chinese Journal of Inorganic Chemistry
基金
国家自然科学基金(No.29631040)
四川省教育厅自然科学基金(No.2000-B33)资助项目。
关键词
纳米超细微粒
固相化学反应
合成
8-羟基喹啉锌
纳米材料
Zn(Oxin)_2·2H_2O(Zinc 8-quinolinolate) nanocrystallite solid state chemical reaction synthesis and characterization
