摘要
目的:建立了检测中国药典中10个阿片系列品种吗啡含量的方法。方法:固相萃取预处理结合高效液相色谱法检测。结果:线性回归、精密度、重复性、回收率等方法学验证均符合规定。结论:方法操作简便,结果准确可靠。
To establish a series methods to analyze the morphine content in 10 species of opium and its preparations. Methods :Samples were purified by C18SPE column and were detormined by HPLC. Results:The calibration curves、average recoveries、precision、accuracy、etc were qualified. Conclution:The method is simple,rapid,accurate and reliable.
出处
《中国药品标准》
CAS
2004年第1期18-21,共4页
Drug Standards of China
关键词
中国药典
阿片类
吗啡
含量测定
固相萃取
高效液相色谱法
opium
a series of preparations containing morphine
morphine
solid phase extraction(SPE)
HPLC
