摘要
以丙烯酸为原料与亚硫酰氯反应得到丙烯酰氯,丙烯酰氯与2,4,6-三溴苯酚在催化剂存在下反应生成丙烯酸三溴苯酯。利用高压液相色谱测定了产品的纯度,达到99.0%以上。利用红外光谱、质谱等测定了产品的结构,与目标化合物完全相符。
The reaction of acrylic acid with thionyl chloride produces acryloyl chloride. Thus, tribromophenyl acrylate is prepared from the reaction of tribromophenol with the as-produced acryloyl chloride in the presence of catalysts. High Pressure Liquid Chromatography analysis gives that the purity of the product is higher than 99.0%. Infrared Spectrum and Mass Spectrum analysis confirms that the structure of the product is just as the same as the expected compound.
出处
《河南科学》
2003年第6期710-712,共3页
Henan Science
