摘要
采用固相合成的方法,首次合成(4S)-1-β-羧乙基-4-羧基杂氮锗三环(1),(4S)-3-甲基1-β-羧乙基-4-羧基杂氮锗三环(2)和(4S)-1-β-羧乙基-4-羧基-2-硫代杂氮锗三环(3).并运用元素分析,IR,1H NMR,MS进行了表征.
(4S)-1-β-carboxyethyl-4-carboxylgermatrane (1). (4S)-3-methyl-1-β-carboxyethyl-4-carboxylgerma-trane (2) and (4S)-1-β-carboxyethyl-4-carboxyl-2-thiogermatrane (3) were synthesized by solid-state reaction of several L-N, N-bis(β-hydroxyethyl) amino-acids with β-trichlorogermapropanic acid and characterized by elemental analysis, IR, 1H NMR and MS spectra.
出处
《有机化学》
SCIE
CAS
CSCD
北大核心
2003年第7期717-719,共3页
Chinese Journal of Organic Chemistry
基金
国家自然科学基金(No.20166001)
