期刊文献+

三氟乙酸修饰TiO_2纳米微粒的制备及磨擦学性能 被引量:1

Preparation and Tribological Properties of TiO_2 Nanoparticles Modified by Trifluoroacetic Acid
下载PDF
导出
摘要 采用化学法制备一种粒径约50nm的三氟乙酸修饰TiO2纳米微粒,并用高分辨透射电镜(HRTEM)、傅立叶红外(FTIR)和热分析(TG、DTA)、X射线粉末衍射(XRD)等手段对该纳米微粒进行了表征,用MRS 10A型四球磨擦试验机考察了该纳米微粒在液体石蜡中的磨擦学性能 结果表明:三氟乙酸修饰TiO2纳米微粒能分散于液体石蜡中且具有较好的抗磨性能,能极大地提高液体石腊的抗磨性和承载能力。 Trifiuoroacetic acidmodified TiO2 nanoparticles with the diameter of 50 nm was prepared using chemical method. The nanoparticles were characterized by a high resolution transmission electron microscope (HRTEM), fourier transformation infrared ray (FTIR) and their thermal stability was investigated by means of thermogravimetric analysis (TG) and differential thermal analysis (DTA).Tribological properties were tested with four ball testing machine. The results showed that the antiwear and load capability of liquid paraffin increased and friction coefficient decreased after adding nanometer TiO2
出处 《化学研究》 CAS 2003年第2期18-20,共3页 Chemical Research
关键词 三氟乙酸修饰TiO2纳米微粒 制备 磨擦学 抗摩性能 润滑添加剂 trifluoroacetic acid TiO_2 nanoparticle luboil additive tribology antiwear ability
  • 相关文献

参考文献3

二级参考文献23

  • 1何勇宁,沈孝良,马礼敦.纳米氧化锌的合成与表征[J].应用化学,1996,13(4):92-94. 被引量:43
  • 2苏宜,谢毅,陈乾旺,钱逸泰.纳米ZnS、CdS水热合成及其表征[J].应用化学,1996,13(5):56-57. 被引量:37
  • 3[1]Zhang Z J, Zhang Z, Xue Q J. Synthesis and Characterization of a Molybdenum Disulfide Nanocluster [J]. J.Phys.Chem.,1994,98,12973. 被引量:1
  • 4[2]Xue Q, Zhang Z, Zhang J. Proceeding of International Tribology conference [C]. Yokohama, Japan, 1995, 366. 被引量:1
  • 5[4]Colthnp N B, Daly I H, Wiberley S E. Introduction to Infrared and Raman Spectroscopy, 3rd ed [M]. San Diego: Academic Press. 1990. 被引量:1
  • 6[5]Morterra C, Orio L, Bolis V, et al. Bi-dimensional Co Cluster at the Surface of Polycrystalline monoclinic ZrO2 [J]. Mater.Chem, Phys.,1991,29:457. 被引量:1
  • 7[6]Severin K G, Archer R D. Characterization of Titanium and Zirconium valerate sol-gel Films [J]. Chem. Mater., 1994, (6):890. 被引量:1
  • 8[7]Deacon G B, Philips R. Rlationships Between The Carbon-oxygen Stretching Frequencies of carboxylate complexes and the type of carboxylate [J]. J Coord Chem Rev, 1980,33:227. 被引量:1
  • 9[8]Doeuff S, Henry M, Sanchez C, et al. Hydrolysis of titanium alkoxides: Modification of the Molecular Precursor by Acetic Acid [J]. J.Non-Cryst.Solids,1987,89:206~216. 被引量:1
  • 10[9]Laaziz I, Larbot A, Julbe A, et al. Hydrolysis of Mixed Titanium and Zirconium Alkoxide by an Esterification Reaction [J]. J.Solid State Chem., 1992,98:393. 被引量:1

共引文献18

同被引文献9

  • 1黄冬根,廖世军,党志.氟掺杂锐钛矿型TiO_2溶胶的制备、表征及催化性能[J].化学学报,2006,64(17):1805-1811. 被引量:37
  • 2沈毅,任富建,刘红娟.掺杂TiO_2的光催化性能研究[J].稀有金属材料与工程,2006,35(11):1841-1844. 被引量:16
  • 3REYES-GARCIA E A, SUN Yanping, REYES-GIL K, et al. ^15N solid state NMR and EPR characterization of N-Doped TiO2 photoeatalysts [J]. Journal of Physical Chemistry C,2007,111 (6) : 2738-2748. 被引量:1
  • 4PINZARI F, PATRONO P, COSTANTINO U. Methanol reforming reactions over Zn/TiO2 catalysts [ J ]. Catalysis Communications,2006,7 (9) :696-700. 被引量:1
  • 5YANG Huaming, SHI Rongrong, ZHANG Ke, et al. Synthesis of WO3/TiO2 nanocomposites via sol-gel method [ J ]. Journal of Alloys and Compounds ,2005,398 (1/2) : 200 -202. 被引量:1
  • 6LUO Xinshi, ZHA Congji, LUTHER DAVIES B. Photosensitivity of titania-doped hybrid polymer prepared by an anhydrous sol-gel process [ J ]. Optical Materials, 2005, 27 (8) : 1461-1466. 被引量:1
  • 7YU J C, YU Jiaguo, HOW K, et al. Effects of F-doping on the photocatalytic activity and microstructures of nanocrystalline TiO2 powders [ J ]. Chem Mater,2002,14 (9) : 3808-3816. 被引量:1
  • 8YU J C, HOW K, YU Jiaguo, et al. Effects of trifluoroacetic acid modification on the surface microstructures and photocatalytic activity of mesoporous TiO2 thin films [J]. Langmuir,2003,19(9):3889-3896. 被引量:1
  • 9KAWAMOTO Y, OGURA K, SHOJIYA M, et al, Fls XPS of fluoride glasses and related fluoride crystals [ J ]. Journal of Fluorine Chemistry, 1999,96 (2) : 135-139. 被引量:1

引证文献1

二级引证文献8

相关作者

内容加载中请稍等...

相关机构

内容加载中请稍等...

相关主题

内容加载中请稍等...

浏览历史

内容加载中请稍等...
;
使用帮助 返回顶部