摘要
利用正交法对d - 艹宁 烯合成L -香芹酮的第二步 (脱氯化氢 )和第三步 (水解反应 )反应的工艺条件进行分析 ,得到了较为理想的工艺 ,使二、三两步反应总收率达 80 %以上。
The second and the third step reaction conditions of the synthesis of L-carvone from d-limonene were studied by the use of orthogonal design, and the whole yield of these two reactions is more than 80% by the use of new reaction conditions.
出处
《天津化工》
CAS
2003年第2期38-39,54,共3页
Tianjin Chemical Industry
关键词
d-苧烯
L-香芹酮
合成
正交
d-limonene
L-carvone
synthesis
orthogonal design
