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湿法快速消解-原子荧光光谱法测定蔬菜中的总砷

Determination of Total Arsenic in Vegetables by Wet Rapid Digestion Atomic Fluorescence Spectrometry
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摘要 本文建立湿法快速消解-原子荧光光谱法测定蔬菜中的总砷含量。结果表明,砷浓度在0~10μg·L^(-1)时,方法的线性关系良好,相关系数大于0.999,检出限为0.02μg·L^(-1),回收率为93.3%~102.4%,相对标准偏差为2.9%~4.5%。该方法操作简便,重现性良好,准确可靠。 A fast wet digestion-atomic fluorescence spectrometry method for the determination of total arsenic content in vegetables was developed.The results showed that when arsenic concentration was 0~10μg·L^(-1),the linear relationship was good,the correlation coefficient was greater than 0.999,the detection limit was 0.02μg·L^(-1),the recoveries were 93.3%~102.4%,and the relative standard deviations were 2.9%~4.5%.The method is simple,reproducible,accurate and reliable.
作者 姚烨华 杨荣 YAO Yehua;YANG Rong(Minhang District Agri-Products Quality and Safety Center,Shanghai 201109,China)
出处 《食品安全导刊》 2023年第6期64-66,共3页 China Food Safety Magazine
关键词 湿法快速消解 原子荧光光谱法 蔬菜 总砷 wet fast digestion atomic fluorescence spectrometry vegetables total arsenic
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