摘要
本文介绍了一种3,5-二溴-4-氨基-N-丁基邻苯二甲酰亚胺的合成方法。以4-氨基-N-丁基邻苯二甲酰亚胺为原料,通过溴化法合成3,5-二溴-4-氨基-N-丁基邻苯二甲酰亚胺,并考察了不同溶剂、原料投加量、溴素及双氧水用量、反应温度及反应时间等条件对该反应的影响。
A synthetic process of 3,5-dibromo-4-amino-N-butylphthalimide was introduced in this paper.Using 4-amino-N-butylphthalimide as raw material,3,5-dibromo-4-amino-N-butylphthalimide was synthesized by bromination method.The effects of different solvents,raw material dosage,bromine and hydrogen peroxide dosage,reaction temperature and reaction time on the reaction were investigated.
作者
丁兴成
高立江
宋龙锋
章文刚
陈海滨
何江伟
DING Xing-cheng;GAO Li-jiang;SONG Long-feng;ZHANG Wen-gang;CHEN Hai-bin;HE Jang-wei(Zhejiang Runtu Co.,Ltd.,Shaoxing 312369,Zhejiang China)
出处
《染料与染色》
CAS
2022年第5期41-43,共3页
Dyestuffs and Coloration
基金
浙江省万人计划科技创新领军人才资助项目(2019R52058)。
