摘要
热脱附-气质联用法作为一种无损分析技术,可以用于测定函套中的挥发性物质。为此,用Tenax-TA吸附管对10种目标化合物进行吸附,在优化的色谱条件下,苯、甲苯、乙酸正丁酯、乙苯、间/对二甲苯、苯乙烯、邻二甲苯、正十一烷和糠醛等组分相关性良好。对实际样品进行测定,可以实现函套等装具中挥发性有害物质的分离分析。研究结果对纸质文献的保护有参考作用。
A non-destructive analysis method was established for the determination of volatile substances in folding cases using thermal desorption-gas chromatography/mass spectrometry.Tenax-TA tubes were used for the absorption and desorption of 10 target compounds.Under optimized chromatographic conditions,benzene,toluene,n-butyl acetate,ethylbenzene,m-xylene,p-xylene,styrene,o-xylene,n-undecane and furfural had good linear correlations.Samples in the laboratory were also obtained and analyzed.The results show that separation analysis of volatile hazardous substances can be achieved using this method.
作者
龙堃
易晓辉
田周玲
任珊珊
张铭
LONG Kun;YI Xiaohui;TIAN Zhouling;REN Shanshan;ZHANG Ming(National Library of China, Beijing 100034, China)
出处
《文物保护与考古科学》
北大核心
2020年第6期112-116,共5页
Sciences of Conservation and Archaeology
关键词
热脱附-气质联用
函套
挥发性物质
无损检测
Thermal desorption-gas chromatography/mass spectrometry
Folding case
Volatile substance
Non-destructive analysis
