摘要
以二甲胺(DMA)和烯丙基缩水甘油醚(AGE)为原料合成得到(2-羟基-3-烯丙氧基)丙基二甲基叔胺(AGE-DMA),产品收率可达99.67%。所得化合物结构经过FT-IR和1 H-NMR确认。得出合成AGE-DMA的最优化条件为:n(二甲胺):n(烯丙基缩水甘油醚)=1.00:1.05,反应温度为50℃,反应时间为6h。该方法具有合成工艺简单、反应条件温和产率高等优点,适合工业化生产。
The(2-hydroxy-3-allyloxy)propyl dimethylamine(AGE-DMA)was synthesized using dimethylamine and allyl glycidyl ether as raw materials,the product yield can reach 99.67%.The compounds were characterized and verified by FT-IR and 1 H-NMR.The optimal conditions for the synthesis of AGE-DMA were as follows:n(dimethylamine):n(allylglycidyl ether)=1.00:1.05,the reaction temperature is 50℃,and the reaction time is 6h.The method has the advantages of the synthetic technology was simple,reaction condition was mild,high yield and was suitable for industrialized production.
作者
卢秋晓
汪乔乔
Lu Qiu-xiao;Wang Qiao-qiao(Jiangxi Senior Technical School of Chemical Industry,Jiangxi Nanchang 330039)
出处
《江西化工》
2020年第5期60-62,共3页
Jiangxi Chemical Industry
