摘要
采用王水作为消解液,微波消解-电感耦合等离子体质谱法测定土壤中的锑,方法简便、快速.锑的检出限为0.014mg/kg,相对标准偏差(n=7)为3.44~ 6.98%,该方法用国家一级标准物质验证,结果与标准值相符.
The sample was digested with aqua regia,and Antimony in soil were determined by Microwave digestion-ICP-MS,the method is simple and rapid.The detection limit of the method was 0.014mg/kg,The relative standard deviation(n=7)was 3.44-~6.98%,The analytical results of national primary standard was consonant with standard value.
作者
班雁华
陈桂鸾
黄一帆
Ban Yanhua;Chen Guiluan;Huang Yifan(Guangxi Center for Analysis and Test Research,Nanning 530022)
出处
《现代科学仪器》
2020年第2期69-71,共3页
Modern Scientific Instruments
基金
广西分析测试研究中心基本科研项目:《广西淮山主产区土壤重金属含量分析及淮山安全性研究》(任务书编号:2019ACZ05)。
