摘要
以碱土金属锶的硝酸盐为添加剂,采用"一步法"制备了大小均一、分散性良好的花椰菜状碳酸钙粒子.考察了反应温度、反应时间等因素对碳酸钙结晶行为的影响,确定了最佳反应条件.利用扫描电子显微镜(SEM)、X射线衍射仪(XRD)、X射线能谱仪(EDAX)等对所得产物的结构和性能进行了表征,并探讨了其反应原理.
Strontium nitrate as an additive was added in the system to prepare uniform distributed broccoli-like calcium carbonate particles. The one-step synthetic method was used which is safe and environment-friendly. The resulting calcium carbonate was characterized through scanning electron microscope( SEM),X-ray diffraction( XRD) and energy dispersive X-ray analysis( EDAX). Meanwile,the possible reaction mechanism of calcium carbonate was put forward.
作者
宋云超
赵丽娜
赵芳薇
曹扬
王继库
SONG Yunchao;ZHAO Lina;ZHAO Fangwei;CAO Yang;WANG Jiku(Key Laboratory of Preparation and Application of Environmental Friendly Materials(Jilin Normal University),Ministry of Education,Changchun 130103,China;College of Chemistry,Jilin Normal University,Siping 136000,China)
出处
《高等学校化学学报》
SCIE
EI
CAS
CSCD
北大核心
2019年第10期2046-2051,共6页
Chemical Journal of Chinese Universities
基金
国家自然科学基金(批准号:51404108)资助~~
关键词
碳酸钙
原位制备
沉淀反应
花椰菜状
Calcium carbonate
In situ preparation
Precipitation reaction
Broccoli-like
