摘要
采用硅胶柱色谱及HPLC等色谱技术对兔儿伞全草甲醇提取液正己烷萃取物进行分离纯化,从中分离得到5个单体化合物,经理化性质和波谱数据分析鉴定它们的结构分别为:尼洛替星(1)、羽扇豆酮(2)、羽扇豆醇(3)、β-香树酯醇(4)、24-亚甲基环阿尔廷醇(5),化合物1~5均为首次从兔儿伞中分离得到。
Five compounds were obtained from n-hexane fraction in the methanol extract of the whole herbs of Syneilesis aconitifolia(Bunge)Maxim by silica gel column chromatography and HPLC,and their structures were identified by analysis on their spectral date as nilotecin(1),lupanone(2),lupanol(3),β-amyrin(4),24-methylene cycloaltinol(5).Compounds 1-5 were obtained from the plants for the first time.
作者
王富强
丁娜
王金兰
赵明
李军
张树军
WANG Fu-qiang;DING Na;WANG Jin-lan;ZHAO Ming;LI Jun;ZHANG Shu-jun(College of Chemistry and Chemical Engineering,Qiqihar University,Heilongjiang Qiqihar 161006,China)
出处
《齐齐哈尔大学学报（自然科学版）》
2019年第4期55-57,共3页
Journal of Qiqihar University(Natural Science Edition)
基金
黑龙江省属高等学校基本科研业务费项目(YSTSXK201808)
关键词
兔儿伞
菊科
三萜
Syneilesis aconitifolia(Bunge)Maxim
compositae
triterpenoid
