摘要
目的：建立潜阳育阴颗粒的质量控制方法。方法：以对照药材作为对照,通过薄层色谱法定性鉴别制剂中制何首乌、鬼针草、川牛膝、酒萸肉,用高效液相色谱法测定制剂中制何首乌中二苯乙烯苷的含量。结果：观察发现,在各定性鉴别的薄层色谱中,所鉴别药材的薄层色谱具有明显的特异性,在与对照药材相应的位置上,斑点颜色相同,阴性无干扰。二苯乙烯苷进样浓度在1.3984-179.0μg/mL范围内呈良好的线性关系,r=0.9999,平均回收率98.48%,RSD为1.04%（n=6）。结论：可使用上述方法控制本组制剂质量。
Objective：To establish the quality control standard for Qianyangyuyin Granula.Methods：Spanishneedles Herb,Radix Polygoni Multiflori,Radix Cyathulae,and Fruetus Corni were identified by TLC.A method of HPLC to determine Stilbenes,the main effective component from Radix Polygoni Multiflori,was developed.Results：The studies on the quality control showed that the characteristics for identification by TLC were distinct.The quantification method had the line-arrange of 1.3984 -179.0μg/mL（r=0.9999）.The average recovery was 98.48%and its RSD was 1.04%（n=6）.Conclusion：The methods can be used for the identification and quantification of the preparation..
出处
《亚太传统医药》
2016年第7期24-26,共3页
Asia-Pacific Traditional Medicine
基金
江苏省科技厅社会发展项目(BE2009696)
