摘要
以2,7-二溴芴酮为起始原料,经Suzuki偶合、腙化和1,3-偶极环反应合成了3种新型的含芴基的富勒烯衍生物,其结构经UV-Vis,1H NMR,13C NMR,FT-IR和MALDI-TOF-MS表征。
Three novel [60]fullerene derivatives containing fluorene were synthesized by Suzuki coupling reaction,hydrazone reaction and 1,3-dipolar cycloaddition reaction,using 2,7-dibromofluoren-9-one as the starting material. The structures were characterized by UV-Vis,1H NMR,13 C NMR,FT-IR and MALDI-TOF-MS.
出处
《合成化学》
CAS
CSCD
2016年第3期219-222,共4页
Chinese Journal of Synthetic Chemistry
基金
科技部国际合作项目(2010DFB70470)
