摘要
分别用气相色谱法和液相色谱法测水中硝基苯类。气相色谱法用 ECD 检测器检测，方法检出限为：0.007～0.043μg／L；RSD 在1.4％～5.2％；加标回收率为：91.6％～95.5％；液相色谱法用DAD 检测，方法检出限为：0.09～0.63μg／L；RSD 在0.9％～4.6％；加标回收率为：92.4％～97.2％。气相色谱法根据保留时间定性，液相色谱法根据保留时间和光谱吸收联合定性。
Both GC and HPLC were applied to measure nitrobenzenes content in water.GC uses ECD detector.The lim-its of detection using GC ranged between 0.007 -0.043μg/L.The RSD were between 1.4% ~5.2%.The standard ad-dition recoveries were between 91.6% ~95.5%.HPLC uses DAD detector.The limits of detection were between be-tween 0.09 ~0.63μg/L.The RSD were between 0.9% ~0.9%.The standard recoveries were between 92.4% ~97.2%.The qualitative analysis of GC was based on the retention time.The qualitative analysis of HPLC combined the retention time and the spectral absorption.
出处
《环境科学导刊》
2015年第5期96-99,共4页
Environmental Science Survey
