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Facile synthesis of coordination polymer nanocubes and their conversion into mesoporous single crystal-like Y_2O_3 nanocubes 被引量:1

Facile synthesis of coordination polymer nanocubes and their conversion into mesoporous single crystal-like Y_2O_3 nanocubes
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摘要 Mesoporous single crystal-like Y2O3 nanocubes have been prepared through a coordination-based self- assembly process. Firstly, a uniform nanocube-like Y-lysine precursor was simply prepared with hydrothermal treatment. After the simple thermal treatment process, nanocube-shaped yttrium oxides with the morphology inherited from the Y-lysine precursor were successfully prepared. The phase, morphology, size and crystalline structure were well characterized by XRD, SEM and TEM. N2 adsorption-desorption demonstrates the mesoporous characteristics of the Y2O3 nanocubes, showing a relatively high surface area of 60 m^2/g. Mesoporous single crystal-like Y2O3 nanocubes have been prepared through a coordination-based self- assembly process. Firstly, a uniform nanocube-like Y-lysine precursor was simply prepared with hydrothermal treatment. After the simple thermal treatment process, nanocube-shaped yttrium oxides with the morphology inherited from the Y-lysine precursor were successfully prepared. The phase, morphology, size and crystalline structure were well characterized by XRD, SEM and TEM. N2 adsorption-desorption demonstrates the mesoporous characteristics of the Y2O3 nanocubes, showing a relatively high surface area of 60 m^2/g.
出处 《Chinese Chemical Letters》 SCIE CAS CSCD 2014年第6期869-873,共5页 中国化学快报(英文版)
基金 supported by NSFC(No.21373116) Tianjin Natural Science Research Fund(No.13JCYBJC18300) RFDP(No. 20120031110005) MOE Innovation Team(No.IRT13022) of China
关键词 MESOPOROUS Y2O3 Single crystal Nanocube TEMPLATE-FREE Mesoporous Y2O3 Single crystal Nanocube Template-free
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