摘要
报道了以 DADN(1,5 -二乙酰基 - 3,7-二硝基 - 1,3,5 ,7-四氮杂环辛烷 )为原料在新型硝化剂 N2 O5- HNO3溶液中合成 HMX的方法 ,HMX的得率在 96 %以上 ,熔点 2 72 .0～ 2 72 .8℃。此外 ,对影响 HMX得率的几种因素作了初步分析。
The method of synthesizing HMX is presented in this paper. Using DADN(1,5 diacetyl 3,7-dinitro 1,3,5,7 tetranitrotetrazacycloctane) as reactant, the HMX was synthesized in the nitrating agent of the mixture of dinitrogen pentoxide and nitric acid. The yield of HMX was more than 96%, mp 272.0~272.8℃. In addation, factors that affecting the yield of HMX were discussed preliminely.
出处
《火炸药学报》
CAS
CSCD
2002年第1期45-47,共3页
Chinese Journal of Explosives & Propellants
