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溴氰菊酯胶悬剂的气相色谱分析

Determination of Deltamethrin in the colloidal suspension agent by gas chromatography
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摘要 研究了胶悬剂中溴氰菊酯的浸出方法。采用低固定液涂量、短色谱柱、高柱温 ,气相色谱内标法测定胶悬剂中溴氰菊酯的含量。方法有良好的线性 ,回归方程为Y =0 .5 5 45X +0 .0 2 32 ,相关系数r =0 .9998。方法的RSD为 0 .9% ,回收率 98%~ 10 3% ,精密度和准确性均好。 A method for the determination of Deltamethrin in the colloidal suspension agent by gas chromatography was described.The Deltamethrin was extracted with dichloromethane and then determined by gas chromatography with 0.5 m packed column of 1.5% OV-17 stationary phase and dioctyl didecylate as internal standard. This method recoveries were 98~103 % and the RSD was 0.9%.As the result showed, the method was sensitive and precise for determining Deltamethrin in the colloidal suspension agent.
出处 《贵州师范大学学报(自然科学版)》 CAS 2002年第1期85-86,89,共3页 Journal of Guizhou Normal University:Natural Sciences
关键词 气相色谱法 溴氰菊酯 胶悬剂 含量测定 广谱杀虫剂 色谱柱 回归方程 gas chromatography Deltamethrin colloidal suspension agent
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