摘要
目的：修订完善舒胸胶囊原标准中鉴别及含量测定方法。方法：采用薄层色谱法鉴别三七、红花及高效液相色谱法测定三七中人参皂苷Rg1，Rb1和三七皂苷R。的总量。结果：三七、红花薄层斑点清晰；人参皂苷Rg1，Rb1，三七皂苷R1分别在0．442～11．050μg（r=0．9998）、0．344-8．600μg（r=0．9999）、0．208-5．200μg（r=0．9994）范围内线性关系良好，平均回收率分别为98．97％（RSD为1．4％）、99．57％（RSD为1．8％）、98．58％（RSD为2．2％）。结论：所建方法简便、准确，可用于舒胸胶囊的质量控制。
To improve the methods of identification and assay of Shuxiong Capsules. Methods： Using TLC to identify Ra- dix notoginseng, Flos carthami and HPLC to determine the total contents of ginsenoside RgI , ginsenoside Rbland notoginsenoside R1 of Radix notoginseng. Results： The TLC sports of Radix notoginseng, Flos carthami developed was fairly clear. Ginsenoside RgI , ginsen oside Rb1 and notoginsenoside R1 showed a good linear relationship at the range of 0. 442-11. 050 ug（ r = 0. 9998）, 0. 344-8. 600pug（ r =0. 9999）and 0. 208-5. 200ug（r = 0. 9994）. The average recovery was 98. 97% with RSD 1.4%, 99. 57% with RSD 1.8% and 98.58% with RSD 2. 2%. Conclusion： The method is simple, accurate and can be used to control the quality of Shuxiong Capsules.
出处
《中国药品标准》
CAS
2014年第1期35-38,共4页
Drug Standards of China
