摘要
研究了在11.5 T的磁场强度下,强磁场热处理对稀土-铁基合金TbFe2和Tb0.27Dy0.73Fe1.95的晶体取向、微观形貌及其磁致伸缩性能的影响.结果表明,强磁场退火不会改变合金的择优取向,但是取向度较退火前有显著提高.2种样品的相组成均无变化,但11.5 T热处理使TbFe2样品中的富稀土相明显减少,磁性相面积增大.强磁场热处理后,Tb0.27Dy0.73Fe1.95合金的磁致伸缩系数增幅较小,而TbFe2合金的磁致伸缩系数比无磁场样品有较大提高.
The rare-earth giant magnetostrictive materials are one kind of the most im- portant functional materials now. The rare-earth giant magnetostrictive materials of TbFe2 and Tb0.27Dy0.73Fe1.95（R-Fe） alloys were firstly used in sonar system in military. Now, the applications of these two alloys have been developed widely in both industry and civil fields, such as magne- tomechanical transducers, actuators, adaptive vibration control systems, and so on. The TbFe2 and Tb0.27Dy0.73Fe1.95 alloys both have the Cl5-type cubic Laves phase structure, which has strong mag- netic anisotropy. This causes that the alloys exhibit different magnetostrictive properties along different crystal orientations. So, the preparation of high orientation degree magnetostrictive materials has a great of importance. In this work, it is predicted that the magnetostricive property of these two al- loys can be enhanced with high magnetic field during heat treatment around their Curie and eutectic points. Therefore, a high magnetic field up to 11.5 T was imposed on these two kinds of RFe alloys during heat treatment at different temperatures in the experiments. Then the effects of high magnetic field on the crystal orientation, morphology and magnetostriction were analyzed in detail by XRD, metallographic microscope, and static resistance strain gauge. Also, the relationship between structure and property is discussed. The results showed that high magnetic field didn＇t change the orientation of the R-Fe alloys, but the orientation degree had a great improvement after heat treatment. The phase composition of the two alloys had no change. However, the heat treatment with a magnetic field up to 11.5 T distinctly reduced the rare earth phase of TbFe2 and obviously increased the magnetic phase. In addition, the magnetostrictive property of TbFe2 alloy increased after the heat treatment with high magnetic field. But for Tb0.27Dy0.73Fe1.95 alloy, the magnetostriction was not obviously enhanced. The reason for the improvement of the magnetostricti
出处
《金属学报》
SCIE
EI
CAS
CSCD
北大核心
2013年第9期1148-1152,共5页
Acta Metallurgica Sinica
基金
国家自然科学基金项目51006020
51174056
国家重点基础研究发展计划项目2011CB612206
中央高校基本科研业务费项目N120409001
N120509001资助~~
关键词
强磁场热处理
稀土-铁基合金
磁致伸缩
择优取向
high magnetic field heat treatment, R--Fe alloy, magnetostriction, preferred orientation
