摘要
目的:建立复方莪术油栓中呋喃二烯和莪术醇的含量测定方法。方法:采用《中国药典》2010年版复方莪术油栓〔含量测定〕项下色谱条件。结果:呋喃二烯在85.89～2579.4 ng范围内,莪术醇在16.272～488.16 ng范围内,线性关系良好,平均回收率分别为99%和97%,RSD分别为3.9%与4.0%(n=9)。结论:药典标准色谱条件可同时控制呋喃二烯和莪术醇的含量,为进一步完善复方莪术油栓质量标准提供了参考依据。
Objective： To establish a new method for determination of furanodiene and curcumol in Compound Zedoary Turmeric Oil Suppositories. Method： The determination method of Compound Zedoary Turmeric Oil Suppositories in Ch. P. （edition 2010 ） was a- dopted. Results： The linearity were found in the range of 85.89-2579. 4 ng and 16. 272-488. 16 ng for furanodiene and curcumol re- spectively. The corresponding average recovery were 99% and 97% with RSD 3.9% and 4. 0% （n = 9）. Conclusion： The determi- nation method of Compound Zedoary Turmeric Oil Suppositories in Ch. P. edition 2010 can also determine the contents of furanodiene and curcumol. Thus the method was further improved.
出处
《中国药品标准》
CAS
2013年第2期131-133,共3页
Drug Standards of China
