摘要
以没食子酸甲酯和1-溴代正十六烷为原料,经过醚化和肼解反应,在比较温和的条件下高产率的合成了一种重要的凝胶因子及液晶材料中间体,即标题化合物,并通过红外、核磁和元素分析表征了其结构。
3,4,5-Tris（hexadecyloxy）benzoyl hydrazine,an important intermediate for gelator and liquid crystal,was synthesized by using gallicin and 1-bromine hexadecane as start materials.The title compound was synthesized via etherification and hydrazinolysis reactions under mild reaction conditions with high yield.The title compound was characterized by IR,1HNMR and element analysis.
出处
《化学试剂》
CAS
CSCD
北大核心
2013年第4期367-368,共2页
Chemical Reagents
基金
国家自然科学基金资助项目(21064006
2116-1018)
甘肃省自然科学基金资助项目(1010RJZA018)
教育部长江学者和创新团队发展计划资助项目(IRT1177)
