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石墨烯微波制备的改进及其电化学性能研究 被引量:3

Improvement of microwave for preparation of graphene and research of its electrochemical properties
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摘要 为寻找高效、环保的方法制备出性能优异的石墨烯超级电容器电极,采用制备氧化石墨的改进法得到酸、中性氧化石墨(S-GO、Z-GO),经微波膨胀得到不同形貌的石墨烯纳米片(WS-GO和WZ-GO),对WS-GO活化得样品HWS-GO;通过SEM、FT-IR和电化学工作站对样品的形貌、组成和电化学性能进行表征分析。结果显示:WS-GO比电容可达222 F/g,可逆性好,商业应用潜力大。 In order to find efficient and environmentally friendly method to prepare an excellent performance graphene super capacitor electrode, acidic graphite oxide (S-GO) and neutral graphite oxide (Z-GO) were prepared by the improved synthesis of graphene oxide. After they were expanded by microwave, the different morphologies of graphene nanosheets (WS-GO and WZ-GO) were obtained, and another sample of HWS-GO was also got by activating WS-GO. The composition and morphology of all the samples were studied with SEM, FT-IR, while the electrochemical properties of samples were investigated by using electrochemical workstation. The results indicate that the specific capacitance of the WS-GO is 222 F/g and WS-GO has better reversibility, obvious advantages and huge commercial potential.
出处 《电子元件与材料》 CAS CSCD 北大核心 2013年第4期9-11,15,共4页 Electronic Components And Materials
关键词 超级电容器 石墨烯纳米片 微波 活化 氧化石墨 改进合成 循环伏安法 supercapacitor graphene nanosheet microwave activation grapheme oxide improved synthesis cyclic voltammetry
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