摘要
目的:研究西瓜藤石油醚部位的化学成分。方法:硅胶色谱、聚酰胺色谱分离纯化,根据理化性质和核磁共振结构数据鉴定化合物结构。结果:从西瓜藤乙醇提取物的石油醚萃取部分中共分离得到10个化合物,分别鉴定为β-谷甾醇(β-sitosterol,1)、胡萝卜苷(daucosterol,2)、豆甾醇(stigmasterol,3)、肉豆蔻酸甘油酯(monomyristin,4)、十六烷酸(palmitic acid,5)、棕榈酸甘油酯(monopalmitin,6)、二十二烷酸甘油酯(monobehenin,7)、熊果酸(ursolic acid,8)、二十一烷酸甘油酯(monoheneicosanoin,9)、硬脂酸(stearic acid,10)。结论:化合物1~10均为首次从西瓜藤中分离得到。
Objective: To study the chemical constituents of Citrullus lanatus vine in extracting with petroleum ether. Method: Compounds were isolated and purified by polyamide column chromatography.Their chemical structures were elucidated on the basis of physicochemical properties, and spectral data. Result: Ten compounds were isolated from C. lanatus vine andelucidated as β-sitosterol, daucosterol, stigmasterol, monomyristin, palmitic acid, monopalmitin, monobehenin, ursolic acid, monoheneicosanoin, stearic acid. Conclusion: Compounds of 1-10 were obtained from C. lanatus vine for the first time.
出处
《中国实验方剂学杂志》
CAS
北大核心
2013年第6期131-134,共4页
Chinese Journal of Experimental Traditional Medical Formulae
关键词
西瓜藤
化学成分
石油醚
Citrullus lanatus vine
chemical compounds
petroleum ether