摘要
目的:探讨牛乳中反式脂肪酸(TFA)在不同热处理条件下的变化规律,为工艺参数确立提供依据。方法:采用罗兹-哥特里法提取乳中脂肪,经甲酯化反应后进行气相色谱分析,对牛乳中的TFA含量进行分析比较。结果:在85℃条件下,随着加热时间的延长,牛乳中TFA含量呈显著上升趋势(P<0.05);相同时间内在超高温(T>133℃)条件下,提高灭菌温度,牛乳中TFA含量变化不大(P>0.05);延长灭菌时间,TFA含量明显增加(P<0.05)。结论:以减少TFA生成量为主要依据确立的巴氏杀菌工艺参数是:85℃、15s;UHT工艺参数为(137±2)℃、4s。
Objective: To explore the change rule of the TFA during the processing of pure milk under different heat treatments and to provide a theoretical reference for optimal process parameters. Methods: Trans-fatty acids are extracted with ethanol and petroleum ether from milk, and then methyl-esterificated and analyzed by GC. Results: These results showed that TFA contents revealed an increase as the extension of heating time at 85 ℃ (P〈0.05). The sterilization temperature under UHT (T〉 133℃) condition during the same heating time did not reveal an obvious effect (P〉0.05). TFA revealed an obvious increase with increasing heating time (P〈0.05). Conclusion: The process parameters for controlling the content of TFA required heating temperature of 85 ℃ and heating duration of 15, and industrial pasteurization temperature of(137 ± 2) ℃, heating duration of 4 s under the UHT conditions.
出处
《食品科学》
EI
CAS
CSCD
北大核心
2013年第6期102-105,共4页
Food Science
基金
西北农林科技大学人才基金项目(Z111020923)
关键词
牛乳
不同热处理
反式脂肪酸
气相色谱
milk
different heat treatments
trans-fatty acid
gas chromatography