摘要
以2-甲基-5-硝基苯磺酸、3,4,5-三甲氧基苯甲醛为起始原料,经过缩合、还原等反应,合成标题化合物。通过MS、IR、1HNMR和13CNMR确定了目标化合物的(E)-型结构。
A new compound was synthesized from 2-methyl-5- nitrobenzenesulfonic acid, 3,4,5-trimethoxybenzaldehyde via multiple steps, including condensation and catalytic reduction reaction. The E pattern of the new compound has been determined by mass spectrometry, IR spectra, 1HNMR and 13 CNMR spectroscopy.
出处
《化学试剂》
CAS
CSCD
北大核心
2013年第1期83-84,共2页
Chemical Reagents
