摘要
以二茂铁、甘氨酸为起始原料,经甲酰化、缩合、还原反应制得标题化合物。经元素分析、IR、1HNMR测试确认了其结构,并研究了其合成条件,讨论了溶剂、反应物料的配比、温度和时间等因素对反应体系的影响。
N-Ferrocenylmethyleneglycine was prepared from ferrocene and glycine through a series of reactions, such as formylation, consendation and reduction. The product was characterized by elemental analysis, IR and ^1HNMR. The syn- thesis conditions were studied and the effect factors such as the solvent, molar ratio, temperature and time on the reaction system were discussed.
出处
《化学试剂》
CAS
CSCD
北大核心
2012年第10期949-951,共3页
Chemical Reagents
基金
江西省普通高校重点实验室科研资助项目(GJJ10732)
江西省教育厅科研资助项目(GJJ10608
GJJ09376)
教育部第四批高等学校特色专业建设点资助项目(TS11524)
国家自然科学基金资助项目(21261020)
