摘要
以α 蒎烯为原料 ,通过环氧化和催化异构化得到一种檀香系列的中间体———α 龙脑醛 ,并以化学法及柱层析法对它进行纯化 ,纯度达 95%以上 .该文主要对此过程的反应条件、催化剂用量进行了研究 ,对其分离、提纯方法进行了探索 .
Campholemic Aldehyde,a kind of sandalwood perfume intermediate,was prepared by expoxide and catalytic rearrangement of α pinene.Then it was purified by chemical methods and column development chromatography,whose purity was over 95%.The reaction conditions,the amount of catalyst,the methods of separation and purification in the process were mainly investigated.
出处
《江西师范大学学报（自然科学版）》
CAS
2000年第1期50-53,57,共5页
Journal of Jiangxi Normal University(Natural Science Edition)
基金
江西省自然科学基金资助项目!(982 80 1)
关键词
Α-蒎烯
异构化
纯化
檀香系列香料
中间体
制备
pinene
expoxide
catalytic rearrangement
α campholetic aldehyde
column development chromatography
purification
