Preparation of Silica-bonded Propyl-diethylene-triamine-N- sulfamic Acid as a Recyclable Catalyst for Chemoselective Synthesis of 1,1-Diacetates 被引量：5

Preparation of Silica-bonded Propyl-diethylene-triamine-N- sulfamic Acid as a Recyclable Catalyst for Chemoselective Synthesis of 1,1-Diacetates

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摘要 A simple and efficient procedure for the preparation of silica-bonded propyl-diethylene-triamine-N-sulfamic acid （SPDTSA） by reaction of 3-diethylenetriamine-propylsilica （DTPS） and chlorosulfonic acid in chloroform is described. Silica-bonded propyl-diethylene-triamine-N-sulfamic acid is employed as a recyclable catalyst for the synthesis of 1,1-diacetates from aromatic aldehydes and acetic anhydride under mild and solvent-free conditions at room temperature. Catalyst could be recycled for several times without any additional treatment. A simple and efficient procedure for the preparation of silica-bonded propyl-diethylene-triamine-N-sulfamic acid （SPDTSA） by reaction of 3-diethylenetriamine-propylsilica （DTPS） and chlorosulfonic acid in chloroform is described. Silica-bonded propyl-diethylene-triamine-N-sulfamic acid is employed as a recyclable catalyst for the synthesis of 1,1-diacetates from aromatic aldehydes and acetic anhydride under mild and solvent-free conditions at room temperature. Catalyst could be recycled for several times without any additional treatment.

作者 Nouri Sefat, Maryam Deris, Abdolah Niknam, Khodabakhsh

机构地区 Chemistry Department

出处《Chinese Journal of Chemistry》 SCIE CAS CSCD 2011年第11期2361-2367,共7页 中国化学（英文版）

关键词 silica-bonded propyl-diethylene-triamine-N-sulfamic acid 1 1-diacetates aromatic aldehydes catalyst solvent-free silica-bonded propyl-diethylene-triamine-N-sulfamic acid, 1,1-diacetates, aromatic aldehydes, catalyst, solvent-free

分类号 TQ426.6 [化学工程] TQ925 [轻工技术与工程—发酵工程]

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参考文献37

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Chinese Journal of Chemistry

2011年第11期

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Preparation of Silica-bonded Propyl-diethylene-triamine-N- sulfamic Acid as a Recyclable Catalyst for Chemoselective Synthesis of 1,1-Diacetates 被引量：5

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