摘要
以高沸点溶剂1,4-丁二醇水溶液为萃取剂,以粉碎的花生壳为原料,经煮沸提取木质素,并以固液比、提取时间和醇水体积比为考察因素,采用RSA响应面分析法确定木质素提取的最佳工艺参数,即固液比1∶11,提取时间4 h,醇水体积比95∶5,在此优化工艺下木质素提取率为23.8%。
Lignin was extracted from the broken peanut shell with aqueous solution of 1,4-butanediol as extracting reagent by boiling extraction method.The single-factor extraction tests and response surface analysis were applied to determine the optimum technological condition.The optimum extraction conditions were as follows:the solid-liquid ratio(g/mL)was 1∶11,the extraction time was 4 hours,and the volume ratio of 1,4-butanediol/water was 95∶5.Under this condition,the extraction yield of lignin was 23.82%.
出处
《化学研究与应用》
CAS
CSCD
北大核心
2011年第11期1566-1569,共4页
Chemical Research and Application
关键词
花生壳
木质素
1
4-丁二醇
响应面分析
peanut shell
lignin
1
4-butanediol
response surface analysis